Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 3-Benzyloxyphenylacetonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Sodium Cyanide | HCID 8929 | — |
| 반응물 | 3-(Benzyloxy)benzyl chloride | HCID 13173490 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | 3-Benzyloxyphenylacetonitrile | HCID 519831 | — |
반응 단계
A solution of sodium cyanide (5.9 g.) in dimethyl sulphoxide (40 ml.) was treated with 3-benzyloxybenzyl chloride (23.2 g.) and the reaction mixture stirred and maintained at 60° for 1 hour. The mixture was poured into water and the product was isolated with ether in the usual manner to give 3-benzyloxyphenylacetonitrile, b.p. 162°-166°/0.55 mm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03987158 |
| 출처 데이터셋 | uspto-grants-1976_10 |
| ORD ID | ord-d80b44e9bbcd4bf387415ded71bea0c3 |
| 출처 메모 | uspto-grants-1976_10 |