Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonium Hydroxide → 2-Acetyl-7-chloro-8-sulfamyl-1,2,3,4-tetrahydroisoquinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 반응물 | 2-Acetyl-8-chlorosulfonyl-7-chloro-1,2,3,4-tetrahydroisoquinoline | HCID 12838041 | — |
| 생성물 | 2-Acetyl-7-chloro-8-sulfamyl-1,2,3,4-tetrahydroisoquinoline | HCID 21393800 | — |
반응 단계
2-Acetyl-8-chlorosulfonyl-7-chloro-1,2,3,4-tetrahydroisoquinoline (0.022 mole) is treated with concentrated ammonium hydroxide (30 ml.) with cooling. The resulting solid is filtered off and washed with water to give 2-acetyl-7-chloro-8-sulfamyl-1,2,3,4-tetrahydroisoquinoline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03988339 |
| 출처 데이터셋 | uspto-grants-1976_10 |
| ORD ID | ord-2ee43315900d40d892c042e4c4ba63e7 |
| 출처 메모 | uspto-grants-1976_10 |