참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Benzene | HCID 241 | — |
| 반응물 | Thiophosphoryl chloride | HCID 19883 | — |
| 생성물 | Phenylthionophosphonic dichloride | HCID 19016 | — |
반응 단계
In a 100 cc autoclave, 42.35 g (0.25 mole) of thiophosphoryl trichloride, 19.53 g (0.25 mole) of benzene were charged, and the mixture was heated with stirring at 200° C for 4 hours. The reaction mixture was treated in accordance with the process of Example 1. No phenylphosphonothioic dichloride was produced.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US03988368 |
|---|
| 출처 데이터셋 | uspto-grants-1976_10 |
|---|
| ORD ID | ord-3415756249a948d698066d8c2ad191f4 |
|---|
| 출처 메모 | uspto-grants-1976_10 |
|---|
