Thionyl Chloride → 2-(Chloromethyl)-6-methylnaphthalene
반응식
[CH3:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[CH:8]=[C:7]([CH2:12]O)[CH:6]=[CH:5]2.S(Cl)([Cl:16])=O>C1C=CC=CC=1>[Cl:16][CH2:12][C:7]1[CH:6]=[CH:5][C:4]2[C:9](=[CH:10][CH:11]=[C:2]([CH3:1])[CH:3]=2)[CH:8]=1참가 물질
4
실험 절차
20.3 g. of 6-methyl-2-naphthalenemethanol is dissolved in 100 ml. of dry benzene and to this solution is added 30 ml. of thionyl chloride. The solution is stirred for about one hour and concentrated to yield 2-chloromethyl 6-methylnaphthalene.
후처리
- concentrationconcentrated
출처 및 근거
- ORD 기록
- ord-be97f8851ab442e2a31052c5e03f4ac4
- 출처 데이터셋
- uspto-grants-1976_10
- 특허 번호
- US03988457
반응 노트
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