1,3-Dioctanoyl glycerol → 1,3-Dioctanoyl-2-(2-acetylsalicyloyl)glycerol

HRID 1288598

반응식

HRID 1288598 반응식
[C:1]([C:4]1([OH:13])[CH:12]=[CH:11][CH:10]=[CH:9][CH:5]1[C:6](Cl)=[O:7])(=[O:3])[CH3:2].[C:14]([O:23][CH2:24][CH:25]([CH2:27][O:28][C:29](=[O:37])[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36])[OH:26])(=[O:22])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>>[C:14]([O:23][CH2:24][CH:25]([CH2:27][O:28][C:29](=[O:37])[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36])[O:26][C:6](=[O:7])[CH:5]1[CH:9]=[CH:10][CH:11]=[CH:12][C:4]1([C:1](=[O:3])[CH3:2])[OH:13])(=[O:22])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]

참가 물질

3

반응물 2

HCID 1509111,3-Dioctanoyl glycerolHCID 573615642-Acetylsalicyloyl chloride

생성물 1

HCID 681394871,3-Dioctanoyl-2-(2-acetylsalicyloyl)glycerol수율 71%

실험 절차

In analogy with the preceding examples, 2-acetylsalicyloyl chloride is reacted with 1,3-dioctanoylglycerol which, upon work up as before, yields 71% of the desired 1,3-dioctanoyl-2-(2-acetylsalicyloyl)glycerol as an oil.

출처 및 근거

ORD 기록
ord-c5a9f6850cd0465ba1466b57596eccaf
출처 데이터셋
uspto-grants-1976_10
특허 번호
US03988446

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