Methyl isothiocyanate → HCID 10702319, 화합물

HRID 1289774

반응식

HRID 1289774 반응식
[NH2:1][C:2]1[N:6]=[C:5]([CH3:7])[NH:4][N:3]=1.[CH3:8][N:9]=[C:10]=[S:11]>CN(C)C=O>[NH2:1][C:2]1[N:3]([C:10]([NH:9][CH3:8])=[S:11])[N:4]=[C:5]([CH3:7])[N:6]=1

참가 물질

4

반응물 2

HCID 11167Methyl isothiocyanateHCID 2346103-Amino-5-methyl-4H-1,2,4-triazole

생성물 1

HCID 10702319HCID 10702319, 화합물수율 29%

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

The synthesis method of Example 1-(3) was applied. The compound (664 mg) obtained in (2) above, dimethylformamide (13 ml) and methyl isothiocyanate (600 mg) were used as reagents to give 340 mg of white crystals (yield 29%).

출처 및 근거

ORD 기록
ord-49a7c28491a444d1a3f480263c3ca0df
출처 데이터셋
uspto-grants-1998_05
특허 번호
US05750545

연결된 노트

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