Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Dichloroethane → Methyl 3-(4-chlorophenyl)-2-propenoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Dichloroethane | HCID 11 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2-Propenoic acid, 3-(4-chlorophenyl)- | HCID 15371 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl 3-(4-chlorophenyl)-2-propenoate | HCID 98955 | 95% |
반응 단계
The synthesis method of Example 7-(1) was applied. 4-Chlorocinnamic acid (10.0 g), 1,2-dichloroethane (50 methanol (9.0 ml) and concentrated sulfuric acid (0.4 ml) were used as reagents to give 10.2 g of a white solid (yield 95%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05750545 |
| 출처 데이터셋 | uspto-grants-1998_05 |
| ORD ID | ord-0677265866c244d1aee9377bcdf37155 |
| 출처 메모 | uspto-grants-1998_05 |