Methanol, 1,1-diethoxy-, 1-acetate → HCID 10684276, 화합물

반응식

[NH2:1][C:2]1[N:6]([C:7]([NH:9][CH3:10])=[S:8])[N:5]=[C:4]([NH:11][C:12]([C:14]([O:16][CH2:17][CH3:18])=[O:15])=[O:13])[N:3]=1.[C:19](OC(OCC)OCC)(=O)C>>[C:12]([NH:11][C:4]1[N:3]=[C:2]2[N:1]=[CH:10][N:9]([CH3:19])[C:7](=[S:8])[N:6]2[N:5]=1)([C:14]([O:16][CH2:17][CH3:18])=[O:15])=[O:13]

참가 물질

반응물 2

HCID 84166Methanol, 1,1-diethoxy-, 1-acetate

HCID 86752547HCID 86752547, 화합물

생성물 1

HCID 10684276HCID 10684276, 화합물수율 78%

실험 절차

The synthesis method of Example 55 was applied. The compound (551 mg) obtained in Example 35 and diethoxymethyl acetate (8 ml) were used as reagents. The mixture was reacted at 90° C. for 2 hours to give 442 mg of white powdery crystals (yield 78%).

후처리

customThe synthesis method of Example 55
customThe mixture was reacted at 90° C. for 2 hours

출처 및 근거

ORD 기록: ord-584e223ed1234dba9eb1c5f259aab9df
출처 데이터셋: uspto-grants-1998_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05750545

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