Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester → cis-(+/-)-5-(Azidomethyl)tetrahydro-3-furanthiol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester | HCID 86750331 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 용매 | Sodium methanolate methanol | HCID 23694274 | — |
| 생성물 | cis-(+/-)-5-(Azidomethyl)tetrahydro-3-furanthiol | HCID 86750332 | 64.8% |
반응 단계
The title compound is prepared by the procedure of Example 16 using 0.310 g of product from Example 61 in 4.5 ml of tetrahydrofuran and 0.30 ml of 25% sodium methoxide/methyl alcohol to give 0.159 g of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05750735 |
| 출처 데이터셋 | uspto-grants-1998_05 |
| ORD ID | ord-eec246d0f4684cf9baba81883fabb9e3 |
| 출처 메모 | uspto-grants-1998_05 |