참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Flavanone | HCID 10251 | — |
| 반응물 | Bromine | HCID 24408 | — |
| 반응물 | Bromine flavanone | HCID 131720663 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | 7-Bromo-2-phenyl-chromen-4-one | HCID 466277 | — |
반응 단계
Bromine was added to a solution of flavanone in carbon tetrachloride at 0° C. The ratio of bromine/flavanone was 1.3 in molar terms. The temperature of the solution was raised to 30° C. and kept there for 1 hour. The temperature of the solution was then raised to 65° C. and kept there for 45 minutes.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05756538 |
|---|
| 출처 데이터셋 | uspto-grants-1998_05 |
|---|
| ORD ID | ord-ff6decdcb59d46cd85f25c1ab327ad54 |
|---|
| 출처 메모 | uspto-grants-1998_05 |
|---|
