Ammonium Hydroxide → 2-Chloro-1,3-thiazole-5-sulfonamide
반응식
[Cl:1][C:2]1[S:3][C:4]([S:7](Cl)(=[O:9])=[O:8])=[CH:5][N:6]=1.[NH4+:11].[OH-]>CCN(CC)CC>[Cl:1][C:2]1[S:3][C:4]([S:7]([NH2:11])(=[O:9])=[O:8])=[CH:5][N:6]=1참가 물질
4
실험 절차
Prepared by general procedure III from 2-Chloro-thiazole-5-sulfonyl chloride (1.1 g, 5 mmol) and NH4OH (0.42 mL, 6 mmol) with Et3N (0.77 mL, 6 mmol to give the title compound as alight-brown solid (610 mg, 61%). MS (ISN) 197[(M−H)−.
출처 및 근거
- ORD 기록
- ord-0fcd68ac7d51416db0a6b77d76e03411
- 출처 데이터셋
- uspto-grants-2007_07
- 특허 번호
- US07238808B2
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