Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Bromophenol → p-Bromo-(1-methoxyethoxy)benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Bromophenol | HCID 7808 | — |
| 반응물 | Methyl vinyl ether | HCID 7861 | — |
| 생성물 | p-Bromo-(1-methoxyethoxy)benzene | HCID 22908633 | 90% |
반응 단계
Using p-bromophenol (17.3 g, 0.1 mole) and methyl vinyl ether (14.0 g, 0.2 mole), the reaction was carried out in the same manner as described in Synthesis Example 1, (1), and the crude oil (24 g) was purified by distillation under reduced pressure to afford 20.8 g of p-bromo-(1-methoxyethoxy)benzene as a pale yellow oil having a boiling point 89-90° C./2 mmHg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05468589 |
| 출처 데이터셋 | uspto-grants-1995_11 |
| ORD ID | ord-24808c6fb6474ee0bab5996c316c4c25 |
| 출처 메모 | uspto-grants-1995_11 |