4-Bromophenol → p-Bromo-(1-methoxyethoxy)benzene

HRID 129365

반응식

[CH:1]1[C:6]([OH:7])=[CH:5][CH:4]=[C:3]([Br:8])[CH:2]=1.[CH:9]([O:11][CH3:12])=[CH2:10]>>[Br:8][C:3]1[CH:4]=[CH:5][C:6]([O:7][CH:9]([O:11][CH3:12])[CH3:10])=[CH:1][CH:2]=1

참가 물질

반응물 2

HCID 78084-Bromophenol

HCID 7861Methyl vinyl ether

생성물 1

HCID 22908633p-Bromo-(1-methoxyethoxy)benzene수율 90%

실험 절차

Using p-bromophenol (17.3 g, 0.1 mole) and methyl vinyl ether (14.0 g, 0.2 mole), the reaction was carried out in the same manner as described in Synthesis Example 1, (1), and the crude oil (24 g) was purified by distillation under reduced pressure to afford 20.8 g of p-bromo-(1-methoxyethoxy)benzene as a pale yellow oil having a boiling point 89-90° C./2 mmHg.

후처리

customas described in Synthesis Example 1, (1),
distillationthe crude oil (24 g) was purified by distillation under reduced pressure

출처 및 근거

ORD 기록: ord-24808c6fb6474ee0bab5996c316c4c25
출처 데이터셋: uspto-grants-1995_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05468589

연결된 노트

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