Cyclohexene → HCID 136367440, 화합물

HRID 1295009노트

반응식

[CH:1]1([N:6]2[C:14]([C:15]3[CH:20]=[CH:19][C:18]([O:21]C)=[CH:17][C:16]=3[O:23]C)=[C:13]3[C:8]([C:9]([F:25])=[CH:10][CH:11]=[CH:12]3)=[N:7]2)[CH2:5][CH2:4][CH2:3][CH2:2]1.B(Br)(Br)Br.C1CCCCC=1>>[CH:1]1([N:6]2[C:14]([C:15]3[CH:20]=[CH:19][C:18]([OH:21])=[CH:17][C:16]=3[OH:23])=[C:13]3[C:8]([C:9]([F:25])=[CH:10][CH:11]=[CH:12]3)=[N:7]2)[CH2:2][CH2:3][CH2:4][CH2:5]1

참가 물질

반응물 3

HCID 8079Cyclohexene

HCID 25134Boron tribromide

HCID 68884042HCID 68884042, 화합물

생성물 1

HCID 136367440HCID 136367440, 화합물수율 44.5%

실험 절차

Prepared according to Method D step C from 2-cyclopentyl-3-(2,4-dimethoxyphenyl)-7-fluoro-2H-indazole (0.062 g, 0.18 mmol), boron tribromide (0.12 mL, 1.2 mmol) and 1.0 mL of cyclohexene to give the product (0.025 g) as a white solid.

후처리

customPrepared

출처 및 근거

ORD 기록: ord-37755546976245beb0c97b25b2ed48c2
출처 데이터셋: uspto-grants-2007_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07241791B2

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