HCID 22929889, 화합물 → HCID 22929650, 화합물
반응식
[N:1]([CH2:4][C:5]1[C:17]([C:18]#[N:19])=[CH:16][C:8]([C:9]([O:11]C(C)(C)C)=[O:10])=[C:7]([O:20][CH2:21][CH3:22])[CH:6]=1)=[N+:2]=[N-:3]>ClCCl.FC(F)(F)C(O)=O>[N:1]([CH2:4][C:5]1[C:17]([C:18]#[N:19])=[CH:16][C:8]([C:9]([OH:11])=[O:10])=[C:7]([O:20][CH2:21][CH3:22])[CH:6]=1)=[N+:2]=[N-:3]참가 물질
4
실험 절차
After dissolving tert-butyl 4-(azidomethyl)-5-cyano-2-ethoxybenzoate (1.923 g) in dichloromethane (12 ml), trifluoroacetic acid (3 ml) was added while cooling on ice. The mixture was stirred at room temperature for 20 minutes and concentrated. The title compound was obtained as light red crystals.
후처리
- additionwas added
- temperaturewhile cooling on ice
- concentrationconcentrated
출처 및 근거
- ORD 기록
- ord-bdea8125bf704f8a93b3d585594e51a5
- 출처 데이터셋
- uspto-grants-2007_07
- 특허 번호
- US07244730B2
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