HCID 59743051, 화합물 → HCID 69153789, 화합물

반응식

[CH2:1]([O:3][CH2:4][N:5]1[C:9]2=[N:10][C:11]3[N:12]([CH3:26])[C:13](=[O:25])[N:14]([CH2:18][CH2:19][CH2:20][CH2:21][C@H:22]([OH:24])[CH3:23])[C:15](=[O:17])[C:16]=3[N:8]2[CH2:7][CH2:6]1)[CH3:2].C(O[C@@H](C)CCCCCl)(=O)C>>[CH2:1]([O:3][CH2:4][N:5]1[C:9]2=[N:10][C:11]3[N:12]([CH3:26])[C:13](=[O:25])[N:14]([CH2:18][CH2:19][CH2:20][CH2:21][C@@H:22]([OH:24])[CH3:23])[C:15](=[O:17])[C:16]=3[N:8]2[CH2:7][CH2:6]1)[CH3:2]

참가 물질

반응물 2

HCID 59743051HCID 59743051, 화합물

HCID 69155336HCID 69155336, 화합물

생성물 1

HCID 69153789HCID 69153789, 화합물

실험 절차

(S)-7,8-dihydro-8-ethoxymethyl-3-(5-hydroxyhexyl)-1-methyl-1H-imidazo[2,1-f]-purine-2,4(3H,6H)-dione was prepared according to the method described for the synthesis of (R)-7,8-dihydro-8-ethoxymethyl-3-(5-hydroxyhexyl)-1-methyl-1H-imidazo[2,1-f]-purine-2,4(3H,6H)-dione but using (S)-5-acetoxy-1-chlorohexane in place of (R)-5-acetoxy-1-chlorohexane.

출처 및 근거

ORD 기록: ord-9791fe4bfa9744aa984131962c09bf9f
출처 데이터셋: uspto-grants-2007_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07247630B2

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