Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl Alcohol → Allyl 4-hydroxy-3-methoxybenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl Alcohol | HCID 7858 | — |
| 반응물 | Vanillic Acid | HCID 8468 | — |
| 용매 | Sulfuric Acid | HCID 1118 | — |
| 생성물 | Allyl 4-hydroxy-3-methoxybenzoate | HCID 11117259 | 75% |
반응 단계
In a manner analogous to Example 1(a), 5 g (30 mmoles) of 4-hydroxy-3-methoxybenzoic acid treated at 100° C. for 4 hours with 50 ml of allyl alcohol and 820 μl of concentrated sulfuric acid, give 4.65 g (75% yield) of the expected ester in the form of a slightly yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05468897 |
| 출처 데이터셋 | uspto-grants-1995_11 |
| ORD ID | ord-877c07731dfd4847a8cf610d152a9e72 |
| 출처 메모 | uspto-grants-1995_11 |