Hexacyanocobalt → HCID 11125012, 화합물

HRID 129704노트

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HRID 129704 반응식
[C-:1]#[N:2].[C-]#N.[C-]#N.[C-]#N.[C-]#N.[C-]#N.[Co:13].[Cl-].[Zn+2:15].[Cl-]>O>[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[Co+3:13].[Co+3:13].[Zn+2:15].[Zn+2:15].[Zn+2:15]

참가 물질

4

반응물 2

HCID 407334HexacyanocobaltHCID 3007855Zincchloride

생성물 1

HCID 11125012HCID 11125012, 화합물

시약·촉매·용매 1

HCID 962Water용매3회

실험 절차

Potassium hexacyanocobaltate (4.0 g) is dissolved in deionized water (150 mL) in a beaker. Zinc chloride (10 g) is dissolved in deionized water (15 mL) in a second beaker. The aqueous solutions are quickly combined and magnetically stirred for 10 min. The precipitated solids are isolated by centrifugation. The solids are reslurried in deionized water (100 mL) for 10 min. with stirring, and are again recovered by centrifugation. The catalyst is dried in a vacuum oven at 50° C. and 30 in. (Hg) to constant weight. This catalyst is identified as Catalyst A.

후처리

  1. customThe precipitated solids are isolated by centrifugation
  2. stirringwith stirring
  3. customare again recovered by centrifugation
  4. customThe catalyst is dried in a vacuum oven at 50° C.

출처 및 근거

ORD 기록
ord-4c4d4bd84224447f98312cdde1f2fee1
출처 데이터셋
uspto-grants-1995_11
특허 번호
US05470813

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