Piperazine → 1-[2-(Diphenylmethoxy)ethyl]piperazine

HRID 129733노트

반응식

HRID 129733 반응식
[C:1]1([CH:7]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[O:8][CH2:9][CH2:10]Cl)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH:18]1[CH2:23][CH2:22][NH:21][CH2:20][CH2:19]1>>[C:1]1([CH:7]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[O:8][CH2:9][CH2:10][N:18]2[CH2:23][CH2:22][NH:21][CH2:20][CH2:19]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

3

반응물 2

HCID 4837PiperazineHCID 141724Benzhydryl 2-chloroethyl ether

생성물 1

HCID 6485251-[2-(Diphenylmethoxy)ethyl]piperazine수율 75%

실험 절차

Following a procedure similar to that described in Preparation 5(c), but using 2-(diphenylmethoxy)ethyl chloride and anhydrous piperazine, the title compound was obtained in a yield of 75%.

출처 및 근거

ORD 기록
ord-b8dc7c77972e4c0cad0ccab8ac739fe3
출처 데이터셋
uspto-grants-1995_11
특허 번호
US05470851

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