N-(3,4-Dichlorophenyl)thiourea → HCID 32253410, 화합물

HRID 130357

반응식

HRID 130357 반응식
Br[CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([S:11]([CH3:14])(=[O:13])=[O:12])=[CH:7][CH:6]=1)=O.[Cl:15][C:16]1[CH:17]=[C:18]([NH:23][C:24]([NH2:26])=[S:25])[CH:19]=[CH:20][C:21]=1[Cl:22]>>[Cl:15][C:16]1[CH:17]=[C:18]([NH:23][C:24]2[S:25][CH:2]=[C:3]([C:5]3[CH:10]=[CH:9][C:8]([S:11]([CH3:14])(=[O:13])=[O:12])=[CH:7][CH:6]=3)[N:26]=2)[CH:19]=[CH:20][C:21]=1[Cl:22]

참가 물질

3

반응물 2

HCID 710776N-(3,4-Dichlorophenyl)thioureaHCID 7358232-Bromo-4'-(methylsulfonyl)acetophenone

생성물 1

HCID 32253410HCID 32253410, 화합물수율 78%

실험 절차

(3,4-Dichloro-phenyl)-[4-(4-methanesulfonyl-phenyl)-thiazol-2-yl]-amine was prepared in 78% yield using the procedure described in example 31 from 2-Bromo-1-(4-methanesulfonyl-phenyl)-ethanone and (3,4-Dichloro-phenyl)-thiourea. 1H NMR (300 MHz, DMSO-d6) δ 8.16-7.56 (m, 8H), 3.24 (s, 3H).

출처 및 근거

ORD 기록
ord-d8b297154fbb4023a7544f427b415052
출처 데이터셋
uspto-grants-2008_06
특허 번호
US07381736B2

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