Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Peroxide → 3-(4-Formyl-phenoxymethyl)-benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Peroxide | HCID 784 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 3-[(4-Formylphenoxy)methyl]benzonitrile | HCID 17608676 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | 3-(4-Formyl-phenoxymethyl)-benzamide | HCID 47172831 | — |
반응 단계
To a solution of 3-(4-Formyl-phenoxymethyl)benzonitrile (1 equiv), in DMSO was added potassium carbonate (0.5 equiv), and hydrogen peroxide (4 equiv). The reaction mixture stirred at room temperature for 2 hours. The reaction was monitored by TLC. It was poured on water and extracted with ethyl acetate (×3). The organic phase was dried over magnesium sulphate, filtered and concentrated under vacuum to yield a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07381750B2 |
| 출처 데이터셋 | uspto-grants-2008_06 |
| ORD ID | ord-b846b8b452874160bf4fee4b5eca3a8f |
| 출처 메모 | uspto-grants-2008_06 |