Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chloro-2-nitroaniline → 2-(4-Chloro-2-nitro-phenylamino)-5-trifluoromethyl-benzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chloro-2-nitroaniline | HCID 6979 | — |
| 반응물 | 2-Fluoro-5-(trifluoromethyl)benzonitrile | HCID 521016 | — |
| 생성물 | 2-(4-Chloro-2-nitro-phenylamino)-5-trifluoromethyl-benzonitrile | HCID 58625992 | 95% |
반응 단계
Using a method similar to Example 39, using 4-chloro-2-nitro-phenylamine (6.4 g, 37.3 mmol), 2-fluoro-5-trifluoromethyl-benzonitrile (7.05 g, 37.3 mmol) to obtain 12.03 g of the title compound (95% yield) as an amorphous yellow solid. Product can be used as is with no further purification: Mass Spectrum (m/e): 342(M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07384934B2 |
| 출처 데이터셋 | uspto-grants-2008_06 |
| ORD ID | ord-3b5cb89fabd84709bb6d39d0840549fc |
| 출처 메모 | uspto-grants-2008_06 |