Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formic Acid → 1,2-Dodecanediol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | Hydrogen Peroxide | HCID 784 | — |
| 반응물 | 1-Dodecene | HCID 8183 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1,2-Dodecanediol | HCID 92866 | — |
반응 단계
336 g (2.00 mol) of 1-dodecene were reacted with 236 g of formic acid and 185 g of a 50% strength aqueous H2O2 solution in accordance with Example 4. 412 g of ethanol were employed for the Marlon AS3 acid-catalyzed transesterification, and the main fraction obtained after the workup by distillation was 99.5% pure, virtually odorless 1,2-dodecanediol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07385092B2 |
| 출처 데이터셋 | uspto-grants-2008_06 |
| ORD ID | ord-e3f2b7809e3f48e28f4d2541ab2247dc |
| 출처 메모 | uspto-grants-2008_06 |