Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 13326생성일: 2026년 10월 25일
Dimethylformamide → N-(4-benzyloxy-5-(2-fluorophenoxy)-2-nitrophenyl)pyrazinecarboxamide
https://huagongshe.com/reaction/13326
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | 2-Fluorophenol | HCID 9707 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | N-(4-benzyloxy-5-fluoro-2-nitrophenyl)pyrazinecarboxamide | HCID 23145743 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-(4-benzyloxy-5-(2-fluorophenoxy)-2-nitrophenyl)pyrazinecarboxamide | HCID 23145658 | — |
반응 단계
0.54 ml of 2-fluorophenol and 2.53 g of potassium carbonate were added to a dimethylformamide (16 ml) solution of 2.14 g of N-(4-benzyloxy-5-fluoro-2-nitrophenyl)pyrazinecarboxamide, and the reaction liquid was stirred at 90° C. for 5 hours, and then water was added to it. The resulting deposit was taken out through filtration to obtain the entitled compound as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07728025B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_06 |
|---|
| ORD ID | ord-76da9412acef46d08b316ba9c7c4c87c |
|---|
| 출처 메모 | uspto-grants-2010_06 |
|---|
