Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isobutyl iodide → 1,3-dihydro-1-isobutyl-5-phenyl-2H-1,4-benzodiazepin-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isobutyl iodide | HCID 10556 | — |
| 반응물 | RO-05-2921 | HCID 76175 | — |
| 생성물 | 1,3-dihydro-1-isobutyl-5-phenyl-2H-1,4-benzodiazepin-2-one | HCID 22312025 | — |
반응 단계
1,3-Dihydro-5-phenyl-2H-1,4-benzodiazepin-2-one (prepared according to the procedure of M. G. Bock et al., J. Org. Chem. 1987, 52, 3232-3239) was alkylated with isobutyl iodide using General Procedure 8-G to afford 1,3-dihydro-1-isobutyl-5-phenyl-2H-1,4-benzodiazepin-2-one.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07390801B2 |
| 출처 데이터셋 | uspto-grants-2008_06 |
| ORD ID | ord-130745f3862e46b4a7d3cb95f03b50b4 |
| 출처 메모 | uspto-grants-2008_06 |