Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,4-Dichloroaniline → N-(3,4-dichlorophenyl)alanine Benzyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,4-Dichloroaniline | HCID 7257 | — |
| 반응물 | Benzyl 2-oxopropanoate | HCID 11769098 | — |
| 생성물 | N-(3,4-dichlorophenyl)alanine Benzyl Ester | HCID 15434839 | — |
반응 단계
Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and benzyl pyruvate (prepared by following General Procedure AO above using benzyl alcohol in place of iso-butanol), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.4 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07390801B2 |
| 출처 데이터셋 | uspto-grants-2008_06 |
| ORD ID | ord-53ad6f4396d240da98f23cb42cff3379 |
| 출처 메모 | uspto-grants-2008_06 |