Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-Butyl bromoacetate → N-(3,4-dichlorophenyl)alanine Tert-butyloxycarbonylmethyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-Butyl bromoacetate | HCID 79177 | — |
| 반응물 | N-(3,4-dichlorophenyl)alanine | HCID 5491659 | — |
| 생성물 | N-(3,4-dichlorophenyl)alanine Tert-butyloxycarbonylmethyl Ester | HCID 54406316 | — |
반응 단계
Following General Procedure AE above and using N-(3,4-dichlorophenyl)alanine (from Example AB above) and tert-butyl bromoacetate (Aldrich), the title compound was prepared as a solid. The reaction was monitored by silica gel tlc (Rf=0.57 in 25% EtOAc/hexanes). Purification was by recrystallization from ethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07390801B2 |
| 출처 데이터셋 | uspto-grants-2008_06 |
| ORD ID | ord-ef0c7234d0d342eba5bf718543a66269 |
| 출처 메모 | uspto-grants-2008_06 |