Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,3'-Bis(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-4,4'-oxydianiline → 4,4'-Diaminodiphenyl Ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,3'-Bis(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-4,4'-oxydianiline | HCID 86623391 | — |
| 반응물 | 3-(1-Hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-4,4'-oxydianiline | HCID 86623392 | — |
| 생성물 | 4,4'-Diaminodiphenyl Ether | HCID 7579 | 12.2% |
| 생성물 | Hexafluoroacetone | HCID 12695 | — |
반응 단계
The reaction liquid was found by gas chromatography (GC) analysis to contain 56.2% of the target compound, 3-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-4,4′-oxydianiline, 22.4% of 3,3′-bis(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-4,4′-oxydianiline, 9.1% of an imine produced by the reaction of hexafluoroacetone with the amine moiety of 4,4′-oxydianiline, and 12.2% of 4,4′-oxydianiline. 50 ml of toluene and 50 ml of water were added to the reaction liquid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728103B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-2472eabbe1b94b06bb753bf3c6653762 |
| 출처 메모 | uspto-grants-2010_06 |