Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 178488270, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Ethyl xanthate | HCID 8823 | — |
| 반응물 | 2-Amino-4-methoxyphenol | HCID 1419108 | — |
| 반응물 | Potassium | HCID 5462222 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 178488270 | HCID 178488270 | — |
반응 단계
The mixture containing 2-amino-4-methoxyphenol (1 eq) and O-ethylxanthic acid, potassium salt (1.1 eq) in pyridine was refluxed for two hours. The resultant mixture was poured in to ice/water containing hydrochloric acid to yield a 5-methoxybenzoxazole-2-thiol as a tan solid. MS: MH+=182
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728010B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-1ba58c26ef34430b9490f5d46f38e4d4 |
| 출처 메모 | uspto-grants-2010_06 |