1-Ethyl-4-(4-nitrophenyl)piperazine → 4-(4-Ethylpiperazin-1-yl)aniline

HRID 13479

반응식

HRID 13479 반응식
[CH2:1]([N:3]1[CH2:8][CH2:7][N:6]([C:9]2[CH:14]=[CH:13][C:12]([N+:15]([O-])=O)=[CH:11][CH:10]=2)[CH2:5][CH2:4]1)[CH3:2]>CO.[Pd]>[CH2:1]([N:3]1[CH2:4][CH2:5][N:6]([C:9]2[CH:14]=[CH:13][C:12]([NH2:15])=[CH:11][CH:10]=2)[CH2:7][CH2:8]1)[CH3:2]

참가 물질

4

반응물 1

HCID 28575491-Ethyl-4-(4-nitrophenyl)piperazine

생성물 1

HCID 9367384-(4-Ethylpiperazin-1-yl)aniline

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 887Methanol용매

실험 절차

The mixture containing 4-ethyl-1-(4-nitrophenyl)piperazine in methanol with catalytic amount of 10% Pd/C was hydrogenated to yield 4-(4-ethylpiperazinyl)phenylamine. MS: MH+=205.

출처 및 근거

ORD 기록
ord-7dc8a99f75a74d88b13febfbb563aee0
출처 데이터셋
uspto-grants-2010_06
특허 번호
US07728010B2

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