Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Morpholine → 4-[2-(4-Nitrophenyl)ethyl]morpholine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Morpholine | HCID 8083 | — |
| 반응물 | 4-Nitrophenethyl bromide | HCID 79266 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 4-[2-(4-Nitrophenyl)ethyl]morpholine | HCID 2797473 | — |
반응 단계
To 4-(2-bromoethyl)-1-nitrobenzene (1 eq) in tetrahydrofuran was added morpholine (3 eq) and stir for 16 h at ambient temperature. Concentrating and passing through a plug of silica gave 4-[2-(4-nitrophenyl)ethylmorpholine. MS: MH+=236.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728010B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-6a95f2b711a1461a8fd21c53214e6a68 |
| 출처 메모 | uspto-grants-2010_06 |