Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Benzenediol, 4-(2-amino-1-hydroxyethyl)- → HCID 131726384, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Benzenediol, 4-(2-amino-1-hydroxyethyl)- | HCID 951 | — |
| 반응물 | 4-Phenylbenzoyl chloride | HCID 84151 | — |
| 반응물 | (2S,4EZ)-1(tert-butoxycarbonyl)-4-(methoxyimino)-2-pyrrolidinecarboxylic acid | HCID 58714586 | — |
| 생성물 | HCID 131726384 | HCID 131726384 | — |
반응 단계
Following the general method as outlined in Example 22, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-(methoxyimino)-2-pyrrolidinecarboxylic acid, [1,1′-biphenyl]-4-carbonyl chloride, and 4-[(1RS)-2-amino-1-hydroxyethyl]-1,2-benzenediol, the title compound was obtained in 66% purity by HPLC. MS(ESI+): m/z=490.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07211601B2 |
| 출처 데이터셋 | uspto-grants-2007_05 |
| ORD ID | ord-9131700a2fb34a4f91c51b702f009bdc |
| 출처 메모 | uspto-grants-2007_05 |