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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1349823생성일: 2026년 10월 27일

Triethylamine → N-(3-{1-Perhydro-2H-pyran-2-yl-5-[1-(triphenylmethyl)(1,2,4-triazol-3-yl)](1H-indazol-3-yl)}phenyl)-3-phenylpropanamide

https://huagongshe.com/reaction/1349823

반응식

참여 물질

역할이름HCID투입량
반응물TriethylamineHCID 8471—
반응물Benzenepropanoyl chlorideHCID 64801—
반응물3-(1-perhydro-2H-pyran-2-yl-5-[1-(triphenylmethyl)(1,2,4-triazol-3-yl)]-1H-indazol-3-yl}phenylamineHCID 21101182—
용매TetrahydrofuranHCID 8028—
생성물N-(3-{1-Perhydro-2H-pyran-2-yl-5-[1-(triphenylmethyl)(1,2,4-triazol-3-yl)](1H-indazol-3-yl)}phenyl)-3-phenylpropanamideHCID 22480348—

반응 단계

To a solution of 3-{1-perhydro-2H-pyran-2-yl-5-[1-(triphenylmethyl)(1,2,4-triazol-3-yl)]-1H-indazol-3-yl}phenylamine (0.150 g, 0.248 mmol) in 2.5 mL of tetrahydrofuran was added 3-phenyl propanoyl chloride (0.084 g, 0.498 mmol), followed by triethyl amine (0.173 mL, 1.24 mmol). The reaction was stirred at room temperature for 2 hours. The reaction mixture was then partitioned between ethyl acetate and water. (Yield not calculated) ES-MS (m/z) 735 [M+H]+.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07211594B2
출처 데이터셋uspto-grants-2007_05
ORD IDord-63f57eec14144b4eb647049f71ad9274
출처 메모uspto-grants-2007_05