Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
O-Xylene → 1,14-Bis(triethoxysilyl)tetradecane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | O-Xylene | HCID 7237 | — |
| 반응물 | Triethoxysilane | HCID 13830 | — |
| 반응물 | Tetradeca-1,13-diene | HCID 30875 | — |
| 반응물 | Vinyl dimethyldisiloxane | HCID 123658807 | — |
| 생성물 | 1,14-Bis(triethoxysilyl)tetradecane | HCID 22559811 | — |
반응 단계
The synthesis method is described in detail by, e.g., H. W. Oviatt et al., Chem. Mater., 1993, 5, 943, and 1,14-bis(triethoxysilyl)tetradecane was synthesized following the above method. A mixture of 25 g of 1,13-tetradecadiene (Aldrich), 44.4 g of triethoxysilane (Shin-etsu Silicones) and 0.1 mL of a 3% xylene solution of platinum complex of bis((vinyl dimethyldisiloxane) (Shin-etsu Silicones) was prepared and stirred at room temperature in a nitrogen atmosphere for 3 days. The reaction effluent was purified by distillation, to obtain 1,14-bis(triethoxysilyl)tetradecane. Its structure was confirmed by NMR analysis.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07214756B2 |
| 출처 데이터셋 | uspto-grants-2007_05 |
| ORD ID | ord-9449d995b31c4cc98ccd3d4b87e0e4be |
| 출처 메모 | uspto-grants-2007_05 |