Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylamine → N,N-dimethyl-5-nitropyridin-2-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | Water | HCID 962 | — |
| 반응물 | 2-Chloro-5-nitropyridine | HCID 78308 | — |
| 용매 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 생성물 | N,N-dimethyl-5-nitropyridin-2-amine | HCID 75707 | — |
반응 단계
2-Chloro-5-nitropyridine (1.0 eq) and dimethylamine (2 M in EtOH, 4.6 eq) in NMP were heated for 2 h at 100° C. The solution was then poured slowly into H2O. The filtrate that formed was filtered and dried to give 2-(dimethylamino)-5-nitropyridine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728010B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-34aaa92fa23d45839859c9f55903dc35 |
| 출처 메모 | uspto-grants-2010_06 |