o-Iodonitrobenzene → HCID 21099425, 화합물

반응식

I[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[N+:8]([O-:10])=[O:9].[F:11][C:12]1[CH:17]=[C:16]([F:18])[CH:15]=[CH:14][C:13]=1[CH2:19][CH2:20][C:21]1[CH:26]=[CH:25][C:24]([S:27](C2C=CC=CC=2)(=[O:29])=[O:28])=[CH:23][CH:22]=1>>[F:11][C:12]1[CH:17]=[C:16]([F:18])[CH:15]=[CH:14][C:13]=1/[CH:19]=[CH:20]/[C:21]1[CH:26]=[CH:25][C:24]([S:27]([C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=2[N+:8]([O-:10])=[O:9])(=[O:29])=[O:28])=[CH:23][CH:22]=1

참가 물질

반응물 2

HCID 69115o-Iodonitrobenzene

HCID 21099424HCID 21099424, 화합물

생성물 1

HCID 21099425HCID 21099425, 화합물

실험 절차

2,4-Difluoro-1-((E)-2-{4-[(2-nitrophenyl)sulfonyl]phenyl}vinyl)benzene was prepared according to the method of Example 135 Step 2 using 2-iodonitrobenzene and Intermediate 2.

출처 및 근거

ORD 기록: ord-32042a47ef79424c91165c4c271cd512
출처 데이터셋: uspto-grants-2007_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07217740B2

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