Acetonitrile → HCID 21889441, 화합물

HRID 1352180노트

반응식

HRID 1352180 반응식
[CH:1]([C:4]1[C:9]([N+:10]([O-:12])=[O:11])=[C:8]([CH:13]([CH3:15])[CH3:14])[CH:7]=[C:6]([CH:16]([CH3:18])[CH3:17])[C:5]=1[S:19]([OH:22])(=[O:21])=[O:20])([CH3:3])[CH3:2].C(#N)C.[Ag:26]=O>CC(C)=O>[CH:1]([C:4]1[C:9]([N+:10]([O-:12])=[O:11])=[C:8]([CH:13]([CH3:14])[CH3:15])[CH:7]=[C:6]([CH:16]([CH3:18])[CH3:17])[C:5]=1[S:19]([O-:22])(=[O:21])=[O:20])([CH3:2])[CH3:3].[Ag+:26]

참가 물질

5

반응물 3

HCID 6342AcetonitrileHCID 92152Silver(II) oxideHCID 218894203-Nitro-2,4,6-tri(propan-2-yl)benzene-1-sulfonic acid

생성물 1

HCID 21889441HCID 21889441, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

Into a flask were charged 20 parts of 2,4,6-triisopropyl-3-nitrobenzenesulfonic acid, 80 parts of acetonitrile and 40 parts of acetone, and the mixture was stirred at room temperature for 16 hours. To this was added 7.46 parts of silver oxide, and the mixture was stirred at room temperature for 16 hours, and then filtered and concentrated to obtain 23.68 parts of silver 2,4,6-triisopropyl-3-nitrobenzenesulfonate.

후처리

  1. stirringthe mixture was stirred at room temperature for 16 hours
  2. filtrationfiltered
  3. concentrationconcentrated

출처 및 근거

ORD 기록
ord-69941d1e013c4be3a0ce3a0526dd9244
출처 데이터셋
uspto-grants-2007_05
특허 번호
US07220532B2

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