Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Anthranilamide → 2-(Phenylamino)Benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Anthranilamide | HCID 6942 | — |
| 반응물 | Bromobenzene | HCID 7961 | — |
| 반응물 | Hexane | HCID 8058 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-(Phenylamino)Benzamide | HCID 96455 | 70% |
반응 단계
Following the general procedure, bromobenzene (55 μL, 0.5 mmol) was coupled with 2-aminobenzamide (102 mg, 0.75 mmol) with the reaction time of 15 h. Chromatography on silica gel column with 1:1 hexane:ethyl acetate gave 74 mg (70%) of the title compound as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07223879B2 |
| 출처 데이터셋 | uspto-grants-2007_05 |
| ORD ID | ord-ac9ec18186204be989636781b1292e6e |
| 출처 메모 | uspto-grants-2007_05 |