참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Azobisisobutyronitrile | HCID 6547 | — |
| 반응물 | Hydroxystyrene | HCID 138202 | — |
| 반응물 | (3-Acryloxypropyl)trimethylsiloxy silane | HCID 131723942 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | hydroxystyrene (3-acryloxypropyl)trimethylsiloxy Silane | HCID 131723941 | — |
반응 단계
15 g (3-acryloxypropyl)trimethylsiloxy silane, 40 g hydroxystyrene and 2.4 g AIBN were dissolved in 80 g THF and charged into a 3-neck flask. The system was then purged with N2 for 30 mins before the temperature was raised to 65° C. The reaction was carried out overnight under N2. On the second day, the solution was precipitated in 2000 mL water. The polymer was collected and dried in vacuum oven overnight at 40° C. The molecular weight was determined by GPC to be 9.1K and the molecular weight showed bimodal distribution.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06586156B2 |
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| 출처 데이터셋 | uspto-grants-2003_07 |
|---|
| ORD ID | ord-e47fe2c4568c40619470eb68d7f38b34 |
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| 출처 메모 | uspto-grants-2003_07 |
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