2-Methoxyethanol → 5-Bromo-4-furan-2-yl-6-(2-methoxy-ethoxy)-pyrimidin-2-yl-amine
반응식
[Br:1][C:2]1[C:3]([C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)=[N:4][C:5]([NH2:11])=[N:6][C:7]=1S(C)=O.[CH3:17][O:18][CH2:19][CH2:20][OH:21].C1CCN2C(=NCCC2)CC1>O1CCOCC1>[Br:1][C:2]1[C:3]([C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)=[N:4][C:5]([NH2:11])=[N:6][C:7]=1[O:21][CH2:20][CH2:19][O:18][CH3:17]참가 물질
5
실험 절차
From 5-bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine, 2-methoxyethanol and DBU in dioxane. ES-MS m/e (%): 316 (M{81Br}+H+, 96), 314 (M{79Br}+H+, 100), 258 ([M{81Br}+H-MeOCH═CH2]+, 70), 256 ([M{81Br}+H-MeOCH═CH2]+, 75).
출처 및 근거
- ORD 기록
- ord-7e6d9f9af5594254aa64198fd9b1d10c
- 출처 데이터셋
- uspto-grants-2003_07
- 특허 번호
- US06586441B2
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