1,8-Diazabicyclo(5.4.0)undec-7-ene → 5-Bromo-4-furan-2-yl-6-(3-phenyl-allyloxy)-pyrimidin-2-yl-amine
반응식
[Br:1][C:2]1[C:3]([C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)=[N:4][C:5]([NH2:11])=[N:6][C:7]=1S(C)=O.[CH2:17]([OH:26])/[CH:18]=[CH:19]/[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1.C1CCN2C(=NCCC2)CC1>O1CCOCC1>[Br:1][C:2]1[C:3]([C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)=[N:4][C:5]([NH2:11])=[N:6][C:7]=1[O:26][CH2:17][CH:18]=[CH:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1참가 물질
5
실험 절차
From 5-bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine, (E)-cinnamyl alcohol and DBU in dioxane. EI-MS m/e (%): 373 (M{81Br}+, 4), 371 (M{79Br}+, 4), 292 ([M—Br]+, 8),202 (14), 117(100), 115 (38),91 (17).
출처 및 근거
- ORD 기록
- ord-ec152ff2678b427db2e13791c87aaaa2
- 출처 데이터셋
- uspto-grants-2003_07
- 특허 번호
- US06586441B2
반응 노트
불러오는 중…