Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → methyl (2S)-4-methyl-2-(methylamino)pentanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 1,4-Dioxane | HCID 31275 | — |
| 반응물 | N-Methylleucine | HCID 2777993 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | methyl (2S)-4-methyl-2-(methylamino)pentanoate | HCID 10921446 | 100% |
반응 단계
N-methyl-L-leucine (1.3 g, 8.95 mmol) was dissolved in 4M HCl, 1,4 dioxane (10 mL) and methanol (10 mL). The solution was stirred overnight at room temperature, then concentrated to afford the title compound as a white solid (100%). MS (ESI): 160.0 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06586466B2 |
| 출처 데이터셋 | uspto-grants-2003_07 |
| ORD ID | ord-c84cddade0974f8e87532868bc68310d |
| 출처 메모 | uspto-grants-2003_07 |