HCID 18504786, 화합물 → HCID 13931389, 화합물
반응식
[C:1]([N:5]([CH3:15])[C:6]1[CH:11]=[CH:10][C:9]([N+:12]([O-])=O)=[CH:8][CH:7]=1)(=[O:4])[CH2:2][CH3:3]>C1COCC1.[Pd]>[C:1]([N:5]([CH3:15])[C:6]1[CH:11]=[CH:10][C:9]([NH2:12])=[CH:8][CH:7]=1)(=[O:4])[CH2:2][CH3:3]참가 물질
4
실험 절차
The reaction is carried out using an analogous method to (9b), using N-propionyl-N-methyl-4-nitroaniline (10a)(6.8 g, 32.86 mmol), 10%Pd on carbon (447 mg) in THF (75 ml). The hydrogenation yields an oil. ES+ (M+1) 178.87.
후처리
- customThe hydrogenation yields an oil
출처 및 근거
- ORD 기록
- ord-d933b64494b546c887d8d9dec84f21ca
- 출처 데이터셋
- uspto-grants-2003_07
- 특허 번호
- US06589950B1
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