Thionyl Chloride → 2-(Chloromethyl)-1,3-dimethoxybenzene

HRID 1357031

반응식

HRID 1357031 반응식
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[C:7]([O:11][CH3:12])[C:4]=1[CH2:5]O.S(Cl)([Cl:15])=O>C1C=CC=CC=1>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[C:7]([O:11][CH3:12])[C:4]=1[CH2:5][Cl:15]

참가 물질

4

반응물 2

HCID 24386Thionyl ChlorideHCID 2776839(2,6-Dimethoxyphenyl)methanol

생성물 1

HCID 127070022-(Chloromethyl)-1,3-dimethoxybenzene

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

0.49 g (2.93 mmol) of 2,6-dimethoxybenzyl alcohol was dissolved in 6 ml of benzene, and the resultant solution was added with 0.41 g (3.32 mmol) of thionyl chloride at a room temperature. The thus obtained solution was then stirred for 1.5 hours at a room temperature to complete a reaction. The reacted solution was then condensed under reduced pressure to obtain a crude product of 2,6-dimethoxybenzyl chloride.

후처리

  1. customa reaction
  2. customcondensed under reduced pressure

출처 및 근거

ORD 기록
ord-18eef18fd527480fadf8042441fb3020
출처 데이터셋
uspto-grants-2003_07
특허 번호
US06589967B1

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