Ammonium Hydroxide → HCID 18506197, 화합물

반응식

[NH2:1][C:2]1[CH:19]=[CH:18][CH:17]=[CH:16][C:3]=1[O:4][C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][CH:13]=1)[C:10](=[O:14])[NH:9][C:8]2=[O:15].[OH-].[NH4+:21]>>[NH2:1][C:2]1[CH:19]=[CH:18][CH:17]=[CH:16][C:3]=1[O:4][C:5]1[CH:6]=[C:7]([C:8]([NH2:21])=[O:15])[C:11](=[CH:12][CH:13]=1)[C:10]([NH2:9])=[O:14]

참가 물질

반응물 2

HCID 14923Ammonium Hydroxide

HCID 18506076HCID 18506076, 화합물

생성물 1

HCID 18506197HCID 18506197, 화합물

실험 절차

5-(2-Aminophenoxy)-isoindole-1,3-dione (0.1 g, 0.38 mmol) in conc. ammonium hydroxide (aq) was stirred at 60° C. for two hours. The reaction mixture was evaporated in vacuo (cold in order not to make the imide again). The crude mixture was used without any purification.

후처리

customThe reaction mixture was evaporated in vacuo (cold in order not
customThe crude mixture was used without any purification

출처 및 근거

ORD 기록: ord-fc642962978f4fe8bbdcf534f802d180
출처 데이터셋: uspto-grants-2003_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06590118B1

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