Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methyl-3-nitrobenzyl alcohol → (3-Amino-4-methylphenyl)methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methyl-3-nitrobenzyl alcohol | HCID 123497 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | (3-Amino-4-methylphenyl)methanol | HCID 586243 | 94.8% |
반응 단계
4-Methyl-3-nitro benzylalcohol (9.7 g, 58 mmol) in ethanol (200 mL) was reduced under 4 atmospheres of hydrogen gas for 4 hours in the presence of 10% Pd/C (0.5 g) to yield after a standard workup 7.54 g (93%) of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06593335B1 |
| 출처 데이터셋 | uspto-grants-2003_07 |
| ORD ID | ord-83dda6c0962d4d169663d0f091c17d1b |
| 출처 메모 | uspto-grants-2003_07 |