Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,1,3-Benzothiadiazol-5-ylmethanol → 2,1,3-Benzothiadiazole-5-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,1,3-Benzothiadiazol-5-ylmethanol | HCID 2776294 | — |
| 촉매 | HCID 178418406 | HCID 178418406 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 2,1,3-Benzothiadiazole-5-carbaldehyde | HCID 2776290 | 72.3% |
반응 단계
5-Hydroxymethylbenzo-2, 1,3-thiadiazole (2.6 g, 16 mmol) and manganese dioxide (6.0 g, 64 mmol) in chloroform (150 mL) were stirred at room temperature overnight. The reaction mixture was filtered off and the filtrate was evaporated to provide 1.9 g of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06593335B1 |
| 출처 데이터셋 | uspto-grants-2003_07 |
| ORD ID | ord-d6214540b07f41f691e40f83b9cf0f40 |
| 출처 메모 | uspto-grants-2003_07 |