Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4,6-Dichloro-5-(o-methoxyphenoxy)-2-methyl-pyrimidine → 5-methyl-N-[6-chloro-5-(o-methoxyphenoxy)-2-methyl-4-pyrimidinyl]-2-pyridine sulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4,6-Dichloro-5-(o-methoxyphenoxy)-2-methyl-pyrimidine | HCID 21979599 | — |
| 반응물 | 5-Methyl-2-pyridine sulfonamide potassium salt | HCID 131723992 | — |
| 생성물 | 5-methyl-N-[6-chloro-5-(o-methoxyphenoxy)-2-methyl-4-pyrimidinyl]-2-pyridine sulfonamide | HCID 22729397 | — |
반응 단계
According to the procedure described in Example 1g) 1.00 g 5-(o-methoxyphenoxy)-4,6-dichloro-2-methyl-pyrimidine was reacted with 5-methyl-2-pyridine sulfonamide potassium salt to give 1.5 g 5-methyl-N-[6-chloro-5-(o-methoxyphenoxy)-2-methyl-4-pyrimidinyl]-2-pyridine sulfonamide. LC-MS: tR=4.57 min, [M+1]+=421.42, [M−1]−=419.46.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06596719B1 |
| 출처 데이터셋 | uspto-grants-2003_07 |
| ORD ID | ord-4e37578a277845f9afcfb41163e55b40 |
| 출처 메모 | uspto-grants-2003_07 |