참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Nitrophenol | HCID 6947 | — |
| 반응물 | Benzyl Chloride | HCID 7503 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Benzyl-2-nitrophenyl Ether | HCID 57359178 | — |
반응 단계
A mixture of 2-nitrophenol (27.82 g˜0.18 mol, Lancaster, contains ca 10% H2O), K2CO3 (33.15 g, 0.24 mol), and benzyl chloride (30.38 g, 27.6 ml, 0.24 mol) was heated at 100° C. for 1.5 h. The resulting mixture was poured in 1.3 L of water and extracted with CHCl3 tree times, washed twice with 50% brine, dried with Na2SO4, filtered and concentrated. Distillation in vacuum gave 39.23 g (96%), bp 161-162° C. (˜0.1 mm Hg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06596734B1 |
|---|
| 출처 데이터셋 | uspto-grants-2003_07 |
|---|
| ORD ID | ord-3f1355235afc4195a10996996216cf34 |
|---|
| 출처 메모 | uspto-grants-2003_07 |
|---|
