Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Bromide → HCID 178515992, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Bromide | HCID 260 | — |
| 반응물 | 2-Benzyl-6-methoxypyridine | HCID 21942274 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178515992 | HCID 178515992 | 70.9% |
반응 단계
A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring for 7 hours in an oil bath kept at 100° C. After cooling as it was, 250 ml of water was added thereto, and the resulting crystals were collected by filtration, washed with water and vacuum-dried, to give 38.9 g of the target compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06599917B1 |
| 출처 데이터셋 | uspto-grants-2003_07 |
| ORD ID | ord-05486037a3b44e6cb1ec2598db258d0c |
| 출처 메모 | uspto-grants-2003_07 |